Electrolysis Synthesis and Characterization Properties of Nickel Oxide Nanoparticle

Authors

  • Yanatra Budi Pramana Industrial Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana Surabaya, Indonesia.
  • Yunia Dwie Nurcahyanie Industrial Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana Surabaya, Indonesia.
  • Muhamad Abdul Jumali Industrial Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana Surabaya, Indonesia.
  • Rhenny Ratnawati Industrial Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana Surabaya, Indonesia.
  • Sugito Sugito Environmental Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana Surabaya, Indonesia.

Keywords:

NiO, Ni(OH)2, Electrolysis Synthesis,

Abstract

Synthesis nickel oxide nanoparticles based on electrolysis method at high voltage (55 V), with concentration natrium citrate optional condition at 0.3 M. The nickel oxide nanoparticles sample were characterized using, X-Ray Diffraction (XRD), Fourier Transform Infrared spectrometer (FTIR), Thermo Gravimetric Analysis (TGA), Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM). XRD result show diffractogram from the product have the same lattice with standard ICDD, Thermogram shows at a temperature above 400 ºC already formed nickel oxide nanoparticles. Spherical nanoparticles were obtained by this method.

References

Saghatforoush, L. A., Hasanzadeh, M., Sanati, S., Mehdizadeh, R. (2012), “Ni(OH)2 and NiO Nanostructures: Synthesis, Characterization and Electrochemical Performance”, Bull, Korean Chem. Soc,Vol. 33, No. 8, 2613.

Khan, Y., Durrani, S.K., Mehmood, M., Jan, A., Abbasi, M.A.(2011), “pH-dependant structural and morphology evolution of Ni(OH)2 nanostructures and their morphology retention upon thermal annealing to NiO”, Journal of Materials Chemistry and Physics, 130 page. 1169– 1174.

Niasari, M. S., Mir, N., Davar, F.(2009), “Synthesis and characterization of NiO nanoclusters via thermal decomposition”, Polyhedron 28, 1111–1114.

Anandan, K., Rajendran, V. (2011), “Morphological and size effects of NiO nanoparticles via solvothermal process and their optical properties”, Materials Science in Semiconductor Processing 14 , 43– 47.

Allagui, A., Wüthrich, R. (2011), “The electrochemical discharges for the synthesis of nickel oxide nanoparticles:Characterization and mechanism”. Electrochimica Acta 58 , 12– 18.

Gondal, M., Saleh, T. A., & Drmosh, Q. (2012),"Synthesis of nickel oxide nanoparticles using pulsed laser ablation in liquids", Applied Surface Science 258, 6982– 6986.

Tahmasian, A., Morsali, A. (2012), “Ultrasonic synthesis of a 3D Ni(II) Metal–organic framework at ambient temperature and pressure: New precursor for synthesis of nickel(II) oxide nano-particles”, Inorganica Chimica Acta 387 , 327–331.

Barani, A., Aghazadeh, M., Ganjali, M. R., Sabour, B., Barmi, A.-A. M., & Dalvand, S. (2014), “Nanostructured nickel oxide ultrafine nanoparticles:Synthesis, characterization, and supercapacitive behavior”. Materials Science in Semiconductor Processing 23 , 85–92.

Budipramana, Y., Suprapto, Ersam, T., Kurniawan, F. (2016), “Influence of CTAB and Sonication on Nickel Hydroxide Nanoparticles Synthesis by Electrolysis at High Voltage”, Lecture Notes in Electrical Engineering , 345-352.

Budipramana, Y., Suprapto, Ersam, T., Kurniawan, F. (2014), “SYNTHESIS NICKEL HIDROXIDE BY ELECTROLYSIS AT HIGH VOLTAGE”, ARPN Journal of Engineering and Applied Sciences

Wu, Z.G., Munoz, M., Montero, O. (2010), “The synthesis of nickel nanoparticles by hydrazine reduction”. Journal of Advanced Powder Technology 2, page. 165–168.

Yan G.X.,and Cheng, D.J.(2007), “Preparation and electrochemical performance of nano-scale nickel hydroxide with different shapes”. Materials Letters 61 , 621–625.,

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Published

2018-05-31

How to Cite

Pramana, Y. B., Nurcahyanie, Y. D., Abdul Jumali, M., Ratnawati, R., & Sugito, S. (2018). Electrolysis Synthesis and Characterization Properties of Nickel Oxide Nanoparticle. Journal of Telecommunication, Electronic and Computer Engineering (JTEC), 10(2-3), 113–116. Retrieved from https://jtec.utem.edu.my/jtec/article/view/4202