Electrolysis Synthesis and Characterization Properties of Nickel Oxide Nanoparticle
Keywords:
NiO, Ni(OH)2, Electrolysis Synthesis,Abstract
Synthesis nickel oxide nanoparticles based on electrolysis method at high voltage (55 V), with concentration natrium citrate optional condition at 0.3 M. The nickel oxide nanoparticles sample were characterized using, X-Ray Diffraction (XRD), Fourier Transform Infrared spectrometer (FTIR), Thermo Gravimetric Analysis (TGA), Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM). XRD result show diffractogram from the product have the same lattice with standard ICDD, Thermogram shows at a temperature above 400 ºC already formed nickel oxide nanoparticles. Spherical nanoparticles were obtained by this method.Downloads
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